Automated atomic absorption determination of lead in gasoline

Automated atomic absorption determination of lead in gasoline

GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY WITH MAlIlRIX MODIFICATION FOR DETERMINATION OF LEAD IN DRINKING WATER

An amoniumvanadate plus sodium molybdate mixed modifier Graphite Furnace Atomic Absorption Spectrometric method has been developed for determination of traces of lead in drinking water. The concentration of lead in the sample is obtained by direct comparison to linear working graph prepared from aqueous standards in the modifier medium, The results indicate the better performance of the pro...

Atomic Absorption Spectrometric Determination of Lead after Extraction and Preconcentration with 5-Br-PADAP

Lead is quantitatively retained on 2-(5-bromo-2-pyridylazo)-5-diethylaminophenol (5-Br-PADAP)-ammonium tetraphenylborate with microcrystalline naphthalene or by a column method in the pH range 4.0-6.0 from a large volume of aqueous solutions of various samples with preconcentration factor of 60. After filtration, the solid mass consisting of the lead complex and naphthalene was dissolved wi...

Determination of lead and cadmium in water samples by cloud point extraction prior to flame atomic absorption spectrometry determination

Pb and Cd in water samples were determined by cloud point extraction (CPE) with sodiumdiethyldithiocarbamate (DDTC) as the chelating agent and octylphenoxypolyethanl (Triton X-114) asthe surfactant prior to flame atomic absorption spectrometry (FAAS) determination. The main factorsof affecting the extraction and detection processes were optimized. The preconcentration of 10 mL ofstandard soluti...

Cold Vapor Atomic Absorption Determination of Hg in Crude Oil and Gasoline Samples after Solid Phase Extraction Using Modified Disks

A facile and highly efficient method have been developed for the preconcentration of the mercury content in crude oil and gasoline samples after digestion with microwave-assisted digestion. Octadecyl silica membrane disk has been modified by the recently synthesized triazene ligand, (E)-1-(2-ethoxyphenyl)-3-(4-nitrophenyl) triaz-1-ene (ENT), then the modified membrane was used for the preco...